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КАТАЛОЖНЫЙ НОМЕР: 361254
Дихлорметан стабилизированный с ~ 20 ppm амилена for Уф, ИК Тест, Вэжх, Гпх, ACS
CH2Cl2
CH2Cl2
M.= 84,93 CAS [75-09-2] EINECS 200-838-9
TARIC 2903 12 00 00
Синонимы: Метилен Хлорид, Метилен Dichloride
PHYSICAL DATA: жидкость, Прозрачная, Бесцветная, Растворяется в вода 20 г/л при 20 °C D 20/4 1,3258 • M.P.: -95 °C • B.P.: 39,75 °C • n20/D : 1,4244 • Темп.вспышкиNO • Темп.горения:605 °C • Vap. press. (20 °C) 453 hPa • Вязк. 20 °C 0,43 mPa.s • D. M. 20 °C 1,6 Дебая • Dielec. constant20 °C 9,1 • Evap. number (DIN 53170) 1,9 • Heat evap. 40 °C 329 KJ/Kg • Satur. conc. 20 °C 1549 g/m3 • Expl. limit14 %(V)25 %(V) •
Библиография: Merck Index 12, 6.140 13, 6.088 Sax MDR000 • Safety 2 , 1140 D • Kühn-Birett M 25 • Ullmann (5.)6 , 235 • Beilstein 1 , 60 I , 8 II , 13 III ,43 IV , 35 • BRN 1730800 • Fieser 1676 2273 4337 7239 • ACS XI • ISO 6353/3-1987 R - 57 , 22 • BP.2018 • USP -NF 36 • Ph. Eur. 8.0 (2014) 9.0 (2017) • F.C.C 10 11 • Directive 88/344/E.C.E.92/115/E.C.E.94/52/EC97/60/EC (27/10/1997) 2009/32/CE • Royal Decree 472/1990 (6/4/1990) , 2667/1998 (11 /12/1998), 1101/2011 (22/7/2011) •
Опасная Доза: C.E: 602-004-00-3 • RTECS: PA 8050000 • LD50 oral rat 2.000 мг/кг • LC50 rat 49000мг/м3 / 7h • LD50 skn rat 2.000 мг/кг • VLA-ED 50 ppm177 мг/м3
Derived No Effect Level (DNEL)
Workers Inhalation, long term (systemic) 706 мг/м3 Workers Dermal, long exposure (systemic) 4750mg/kg Workers Inhalation, long term (systemic) 353 мг/м3 Population Inhalation, acute (systemic) 353 мг/м3 Population, Dermal, long exposure (systemic) 2395mg/kg Population Inhalation, long term (systemic) 88,3 мг/м3 Population, oral, long term (systemic) 0.06mg/kg
Predicted No Effect Концентрация (PNEC)
Freshwater 0.54mg/l Marine вода 0.194mg/l Freshwater Sediment 4.47mg/kg Marine вода Sediment 1.61mg/kg Soil 0.583mg/kg Sewage treatment plant 26mg/l
H: H351 •
P: P201 • P202 • P281 • P308+P313 • P405 • P501 •
ТРАНСПОРТНЫЕ ПОЛОЖЕНИЯ: UN: 1593 • ADR: 6.1/III • IMDG: 6.1/III • IATA: 6.1/III • PAX: 655 • CAO: 663 • (E) •
Вес/ОБЪЕМ: 1l~1,324 kg 1kg~0,755 l
Наблюдения: Хранение away from direct light. •
Спецификация:
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Миним. содержание (Гх.) |
99,9% |
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Плотность при 20/4 |
1,322-1,325 |
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МАКСИМАЛЬНОЕ СОДЕРЖАНИЕ ПРИМЕСЕЙ |
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APHA цвета |
10 |
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Кислотность |
0,0002 мэкв/г |
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Щелочность |
0,0002 мэкв/г |
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Non-летуч. matter |
0,0003 % |
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Хлор (Cl) |
0,0001% |
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Вода (H2O) |
0,01 % |
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Пригодность for ИК спектрометр.: |
passes тест |
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Флуоресценция при 254 nm (по хинину) |
1 ppb |
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Флуоресценция при 365 nm (по хинину) |
1 ppb |
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Уф Spectrum (1cm кювета; Р-р Сравнения: вода): |
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Transmittance при 233 (Cut off) nm |
³ 10 % |
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Transmittance при 235 nm |
³ 40 % |
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Transmittance при 240 nm |
³ 75 % |
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Transmittance при 245 nm |
³ 90 % |
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Transmittance при 255 nm |
³ 98 % |
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Transmittance при 260-400 nm |
³ 99 % |
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Data interest в Вэжх: P' + 0,25 E Rohrschneider Polarity Eluotropic value E° (Al2O3) Sol. H2O в растворителе при 20°C |
5,6 3,1 0,42 0,17 |
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For critical jobs, purge с азот.
Microfiltered product (0.2 µm) и Упакован в атмосфере азота
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PRODUCT CODE: 361254
Dichloromethane stabilized with ~ 20 ppm of amylene for UV, IR, HPLC, GPC, ACS
CH2Cl2
CH2Cl2
M.= 84,93 CAS [75-09-2] EINECS 200-838-9
TARIC 2903 12 00 00
SYNONYMS: Methylene Chloride, Methylene Dichloride
PHYSICAL DATA: liquid, Clear, Colourless, Soluble in water 20 g/l at 20 °C D 20/4 1,3258 • M.P.: -95 °C • B.P.: 39,75 °C • n20/D : 1,4244 • Flash P.:NO • Ign. T.:605 °C • Vap. press. (20 °C) 453 hPa • Viscosity 20 °C 0,43 mPa.s • D. M. 20 °C 1,6 Debye • Dielec. constant20 °C 9,1 • Evap. number (DIN 53170) 1,9 • Heat evap. 40 °C 329 KJ/Kg • Satur. conc. 20 °C 1549 g/m3 • Expl. limit14 %(V)25 %(V) •
BIBLIOGRAPHY: Merck Index 12, 6.140 13, 6.088 Sax MDR000 • Safety 2 , 1140 D • Kühn-Birett M 25 • Ullmann (5.)6 , 235 • Beilstein 1 , 60 I , 8 II , 13 III ,43 IV , 35 • BRN 1730800 • Fieser 1676 2273 4337 7239 • ACS XI • ISO 6353/3-1987 R - 57 , 22 • BP.2018 • USP -NF 36 • Ph. Eur. 8.0 (2014) 9.0 (2017) • F.C.C 10 11 • Directive 88/344/E.C.E.92/115/E.C.E.94/52/EC97/60/EC (27/10/1997) 2009/32/CE • Royal Decree 472/1990 (6/4/1990) , 2667/1998 (11 /12/1998), 1101/2011 (22/7/2011) •
HAZARDOUS: C.E: 602-004-00-3 • RTECS: PA 8050000 • LD50 oral rat 2.000 mg/kg • LC50 rat 49000mg/m3 / 7h • LD50 skn rat 2.000 mg/kg • VLA-ED 50 ppm177 mg/m3
Derived No Effect Level (DNEL)
Workers Inhalation, long term (systemic) 706 mg/m3 Workers Dermal, long exposure (systemic) 4750mg/kg Workers Inhalation, long term (systemic) 353 mg/m3 Population Inhalation, acute (systemic) 353 mg/m3 Population, Dermal, long exposure (systemic) 2395mg/kg Population Inhalation, long term (systemic) 88,3 mg/m3 Population, oral, long term (systemic) 0.06mg/kg
Predicted No Effect Concentration (PNEC)
Freshwater 0.54mg/l Marine water 0.194mg/l Freshwater Sediment 4.47mg/kg Marine water Sediment 1.61mg/kg Soil 0.583mg/kg Sewage treatment plant 26mg/l
H: H351 •
P: P201 • P202 • P281 • P308+P313 • P405 • P501 •
TRANSPORT REGULATIONS: UN: 1593 • ADR: 6.1/III • IMDG: 6.1/III • IATA: 6.1/III • PAX: 655 • CAO: 663 • (E) •
WEIGHT/VOLUME INFORMATION: 1l~1,324 kg 1kg~0,755 l
OBSERVATIONS: Storage away from direct light. •
SPECIFICATIONS:
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Minimum assay (G.C.) |
99,9% |
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Density at 20/4 |
1,322-1,325 |
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Maximum limit of impurities |
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APHA colour |
10 |
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Acidity |
0,0002 meq/g |
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Alkalinity |
0,0002 meq/g |
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Non-volatile matter |
0,0003 % |
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Chlorine (Cl) |
0,0001% |
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Water (H2O) |
0,01 % |
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Suitability for IR spectrometry: |
passes test |
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Fluorescence at 254 nm (as quinine) |
1 ppb |
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Fluorescence at 365 nm (as quinine) |
1 ppb |
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UV Spectrum (1cm cell; Ref.: water): |
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Transmittance at 233 (Cut off) nm |
³ 10 % |
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Transmittance at 235 nm |
³ 40 % |
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Transmittance at 240 nm |
³ 75 % |
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Transmittance at 245 nm |
³ 90 % |
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Transmittance at 255 nm |
³ 98 % |
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Transmittance at 260-400 nm |
³ 99 % |
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Data of interest in HPLC:
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